Note:
“CC” refers to the “Competent Chemist” modules.
“EE” refers to the “Expert Experimentalist” modules.
SES # | LECTURE TOPICS | LAB TOPICS |
---|---|---|
1 | Introductory Lecture, Pre-Lab Reports and Lab Notebooks | Safety Instruments & Check in |
2 | NMR Spectroscopy | CC: Transfer & Manipulation, NMR, IR |
3 | Extraction Techniques & IR Spectroscopy | EE: Acids, Bases & In Between |
4 | Recrystallization Techniques | CC: Recrystallization Mothball |
5 | Mass Spectroscopy | EE: Recrystallization Single Crystal |
6 | Atmospheric & Vacuum Distillation | CC: Distillation, GC and MS |
7 | TLC, Column & Gas Chromatography | EE: Distillation, RI & IR |
8 | Students Present Distillation Results | CC/EE: Column Chromatography |
9 | Protein Assays - Biochemistry | CC: Biochemistry |
10 | Error Analysis | EE: Biochemistry |
11 | Original Research Project Charge, Synthesis of Penicillin Derivatives | Orig Research: Synthesis, Penicillin |
12 | Students Present Results of Synthesis and Schemes | Purify product, Column Chromatography |
13 | Writing Up The Research Lab Report | Test Penicillin with E. Coli |
14 | No Lecture | Complete Research Labwork |
15 | No Lecture | Work on Lab Report |
16 | No Lecture | Work on Lab Report (cont.) |
17 | No Lecture | Lab Reports Due |